HCID 67095900, compound → HCID 57780678, compound

HRID 2076075Notes

Reaction equation

HRID 2076075 reaction equation
CN(C)[CH:3]=[C:4]1[CH2:8][CH2:7][CH:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[C:5]1=O.[N+]([O-])(O)=O.[N+]([O-])(O)=O.[CH3:24][O:25][C:26]1[CH:27]=[C:28]([NH:38][C:39]([NH2:41])=[NH:40])[CH:29]=[CH:30][C:31]=1[N:32]1[CH:36]=[C:35]([CH3:37])[N:34]=[CH:33]1>>[CH3:24][O:25][C:26]1[CH:27]=[C:28]([NH:38][C:39]2[N:41]=[CH:3][C:4]3[CH2:8][CH2:7][CH:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[C:5]=3[N:40]=2)[CH:29]=[CH:30][C:31]=1[N:32]1[CH:36]=[C:35]([CH3:37])[N:34]=[CH:33]1

Participants

3

Reactant 2

HCID 67095900HCID 67095900, compoundHCID 178493228HCID 178493228, compound

Product 1

HCID 57780678HCID 57780678, compound

Procedure

The title compound was prepared from crude ethyl 3-[1-dimethylamino-methylidene]-2-oxo-cyclopentanecarboxylate (70 mg, 0.3 mmol) and N-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-guanidine dinitrate (83 mg, 0.22 mmol) using in analogous manner the procedure described in example 45b). Obtained as a pale-yellow solid (5 mg, 6%). MS ISP (m/e): 394.3 [(M+H)+]. mp 150-153° C.

Sources & evidence

ORD record
ord-8d062e411ce642359a77d9e6d1eb0e2d
Source dataset
uspto-grants-2011_04
Patent number
US07923450B2

Reaction notes

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