tert-Butoxy bis(dimethylamino)methane → HCID 67096124, compound

HRID 2076089Notes

Reaction equation

HRID 2076089 reaction equation
[C:1]([CH:5]1[CH2:10][CH2:9][CH2:8][CH2:7][C:6]1=[O:11])([CH3:4])([CH3:3])[CH3:2].C(O[CH:17](N(C)C)[N:18]([CH3:20])[CH3:19])(C)(C)C>>[C:1]([CH:5]1[CH2:10][CH2:9][CH2:8]/[C:7](=[CH:17]\[N:18]([CH3:20])[CH3:19])/[C:6]1=[O:11])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 79885tert-Butoxy bis(dimethylamino)methaneHCID 1026812-tert-Butylcyclohexanone

Product 1

HCID 67096124HCID 67096124, compound

Procedure

2-tert-Butylcyclohexanone (93 mg, 0.60 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 45a) to give crude title compound (105 mg) as a yellow oil which was used directly in the next step. MS ISP (m/e): 210.2 (100) [(M+H)+].

Sources & evidence

ORD record
ord-d2ce771a611a48dd873c9578a8c61100
Source dataset
uspto-grants-2011_04
Patent number
US07923450B2

Reaction notes

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