HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxy bis(dimethylamino)methane → HCID 67095886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | Ethyl 2-oxocyclohexylacetate | HCID 91229 | — |
| Product | HCID 67095886 | HCID 67095886 | — |
Reaction Steps
Ethyl 2-cyclohexanoneacetate (100 mg, 0.54 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 45a) to give crude title compound (116 mg) as a brown oil which was used directly in the next step. MS ISP (m/e): 194.2 (100) [(M-EtOH+H)+], 240.2 (90) [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-fa0ae2ae473941649756d37d5177202e |
| Source note | uspto-grants-2011_04 |