Cyclohexanone, 2-hydroxy- → HCID 67096264, compound

HRID 2076106Notes

Reaction equation

HRID 2076106 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C:3]1=[O:8].C(O[CH:14](N(C)C)[N:15]([CH3:17])[CH3:16])(C)(C)C>>[CH3:14][N:15]([CH3:17])[CH:16]=[C:7]1[CH2:6][CH2:5][CH2:4][CH:3]([OH:8])[C:2]1=[O:1]

Participants

3

Reactant 2

HCID 10785Cyclohexanone, 2-hydroxy-HCID 79885tert-Butoxy bis(dimethylamino)methane

Product 1

HCID 67096264HCID 67096264, compound

Procedure

2-Hydroxy-cyclohexanone (114 mg, 1.0 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 45a) to give crude title compound (188 mg) as a yellow oil which was used directly in the next step.

Sources & evidence

ORD record
ord-cbb013d812db4858b11cfe00b6e87403
Source dataset
uspto-grants-2011_04
Patent number
US07923450B2

Reaction notes

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