1-Ethyl-1H-imidazole → HCID 131727537, compound

HRID 2076146Notes

Reaction equation

HRID 2076146 reaction equation
[N-:1]([S:9]([C:12]([F:15])([F:14])[F:13])(=[O:11])=[O:10])[S:2]([C:5]([F:8])([F:7])[F:6])(=[O:4])=[O:3].[CH2:16]([N:18]1[CH:22]=[CH:21][N:20]=[CH:19]1)[CH3:17]>>[N-:1]([S:2]([C:5]([F:8])([F:6])[F:7])(=[O:4])=[O:3])[S:9]([C:12]([F:15])([F:14])[F:13])(=[O:11])=[O:10].[CH2:16]([N:18]1[CH:22]=[CH:21][N:20]=[CH:19]1)[CH3:17]

Participants

3

Reactant 2

HCID 815401-Ethyl-1H-imidazoleHCID 4176748N-Propyl-Methyl Piperidinium Bis(trifluoroMethylsulfonyl)Imide

Product 1

HCID 131727537HCID 131727537, compound

Procedure

To 1.0 g of bis(trifluoromethylsulfonyl)imide was added dropwise 0.34 g of N-ethylimidazole in a nitrogen atmosphere in a glove box, and the solution was stirred overnight to obtain N-ethylimidazole bis(trifluoromethylsulfonyl)imide (Etlm+TFSI−) as a colorless transparent liquid. The resulting salt had a melting point of 6.6° C.

Sources & evidence

ORD record
ord-895a1dc2fd1e4315bb65a28ac651f524
Source dataset
uspto-grants-2011_04
Patent number
US07923492B2

Reaction notes

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