Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl 2-hydroxy-6-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]methyl}-3-(trifluoromethyl)benzoate → HCID 67119231, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl 2-hydroxy-6-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]methyl}-3-(trifluoromethyl)benzoate | HCID 67119153 | — |
| 반응물 | HCID 86617418 | HCID 86617418 | — |
| 생성물 | HCID 67119231 | HCID 67119231 | — |
반응 단계
According to a method similar to Example (31) and Example (17-4), from methyl (4-bromophenyl)(ethoxy)acetate (110 mg, 0.4 mmol) and tert-butyl 2-hydroxy-6-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]methyl}-3-(trifluoromethyl)benzoate (170 mg, 0.34 mmol) obtained in Example (22-4), the title compound was obtained as a grayish white powder (35 mg, yield: 19%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07923573B2 |
| 출처 데이터셋 | uspto-grants-2011_04 |
| ORD ID | ord-36d85902171f45029cc0b1b9f40c43b3 |
| 출처 메모 | uspto-grants-2011_04 |