Acetic Acid → HCID 178450750, compound

Participants

Reaction Steps

Tetrakis(triphenylphosphine)palladium (0) (74 mg, 64.4 μmol), acetic acid (0.4 ml, 6.44 mmol) and phenylsilane (0.397 ml, 3.22 mmol) were added to a solution of the mixture (712 mg, 1.29 mmol) obtained in Example (95-3) in methylene chloride (6 ml) under a nitrogen atmosphere, and the mixture was stirred at room temperature for 3 hours. The formed solid was filtered and washed with methylene chloride to give the title compound (469 mg, yield: 71%).

Provenance & Evidence