Acetaminophen → HCID 67108121, compound

HRID 2076719Notes

Reaction equation

HRID 2076719 reaction equation
[CH3:1][C:2]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([OH:11])=[CH:9][CH:10]=1)=[O:3].[N:12]1[CH:17]=[CH:16][C:15]([C:18]2[CH:23]=[CH:22][N:21]=[CH:20][CH:19]=2)=[CH:14][CH:13]=1>O>[CH3:1][C:2]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)=[O:3].[N:12]1[CH:17]=[CH:16][C:15]([C:18]2[CH:23]=[CH:22][N:21]=[CH:20][CH:19]=2)=[CH:14][CH:13]=1.[OH2:3]

Participants

4

Reactant 2

HCID 1983AcetaminophenHCID 111074,4'-Bipyridine

Product 1

HCID 67108121HCID 67108121, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

50 mg (0.3307 mmol) acetaminophen and 52 mg (0.3329 mmol) 4,4′-bipyridine were dissolved in hot water and allowed to stand. Slow evaporation yielded colorless needles of a 1:1:1 acetaminophen/4,4′-bipyridine/water co-crystal, as shown in FIG. 44A-B.

Workup

  1. customSlow evaporation

Sources & evidence

ORD record
ord-70cbbddc818d4a389c281445fd2fa550
Source dataset
uspto-grants-2011_04
Patent number
US07927613B2

Reaction notes

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