HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamazepine → Carbamazepine p-phthalaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | Terephthalaldehyde | HCID 12173 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Carbamazepine p-phthalaldehyde | HCID 131728782 | — |
Reaction Steps
25 mg (0.1058 mmol) carbamazepine and 7 mg (0.0521 mmol) p-phthalaldehyde were dissolved in approximately 3 mL methanol. Slow evaporation of the solvent yielded colorless needles of a 1:1 carbamazepine/p-phthalaldehyde co-crystal, as shown in FIG. 50A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-5dfa08e8a2384fe099b1d551c8fdab9f |
| Source note | uspto-grants-2011_04 |