HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → N-benzoyl-N'-(2-cyanophenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-6-methylbenzonitrile | HCID 279973 | — |
| Product | N-benzoyl-N'-(2-cyanophenyl)thiourea | HCID 909209 | — |
Reaction Steps
Prepared as in example 1a from 2-amino-6-methylbenzonitrile and benzoyl isothiocyanate as a pale-yellow solid. 1H NMR (400 MHz, DMSO-d6) δ 7.40 (m, 1H), 7.52-7.69 (m, 5H), 7.98-8.01 (m, 2H), 11.99 (s, 1H), 12.54 (s, 1H). MS 296 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928111B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-855d2b55fa274c59b62cee09d97eb4a5 |
| Source note | uspto-grants-2011_04 |