HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzonitrile → N-(2-Cyanophenylcarbamoyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzonitrile | HCID 72913 | — |
| Reactant | Benzoyl isocyanate | HCID 78210 | — |
| Product | N-(2-Cyanophenylcarbamoyl)benzamide | HCID 57456910 | — |
Reaction Steps
Prepared as in Example 1a from 2-aminobenzonitrile and benzoyl isocyanate as a white powder (661 mg, 59%). 1H NMR (400 MHz, DMSO-d6) δ 7.27-7.29 (t, 1H), 7.52-7.56 (t, 1H), 7.64-7.74 (m, 2H), 7.82-7.85 (dd, 1H), 8.02-8.04 (m, 2H), 8.22-8.24 (d, 1H). MS 266 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928111B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-c1c85ec0de12405fa27d28f12160dced |
| Source note | uspto-grants-2011_04 |