HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 25222914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 2-Chloro-N,N-dimethylquinazolin-4-amine | HCID 12684342 | — |
| Product | HCID 25222914 | HCID 25222914 | — |
Reaction Steps
Prepared as in Example 46 from 2-chloro-N,N-dimethylquinazolin-4-amine (Example 40) and thiourea. 1H NMR (400 MHz, DMSO-d6) δ 3.31 (s, 6H), 7.24-7.19 (m, 1H), 7.40-7.38 (m, 1H), 7.65-7.61 (m, 1H), 8.00 (d, J=8.0 Hz, 1H), 12.35(s, 1H). MS 206 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928111B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-1de2800a71e84ec7883c202338163836 |
| Source note | uspto-grants-2011_04 |