HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(p-Toluenesulfonylamino)phenylboronic acid pinacol ester → N-(5-(3-(4-methylphenylsulfonamido)phenyl)thiazolo[5,4-b]pyridin-2-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(p-Toluenesulfonylamino)phenylboronic acid pinacol ester | HCID 16217721 | — |
| Reactant | N-(5-Bromothiazolo[5,4-b]pyridin-2-yl)acetamide | HCID 56763853 | — |
| Product | N-(5-(3-(4-methylphenylsulfonamido)phenyl)thiazolo[5,4-b]pyridin-2-yl)acetamide | HCID 57585121 | — |
Reaction Steps
This compound was made using 4-methyl-N-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenesulfonamide and N-(5-bromothiazolo[5,4-b]pyridin-2-yl)acetamide and following the procedure in Example 146, Method N, step 2 above. MS (ESI pos. ion) m/z: 439. Calculated exact mass for C21H18N4O3S2 438.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928140B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-132fef724e1742b795ba27e7161ea7d0 |
| Source note | uspto-grants-2011_04 |