Methyl iodide → HCID 59715670, compound

Participants

Reaction Steps

Potassium carbonate (38.7 mg, 0.280 mmol) and methyl iodide (10.5 μl, 168 mmol) were added to a solution of the compound of Example B245 (15.8 mg, 0.0560 mmol) in dimethylformamide (1 ml), and this reaction mixture was stirred at room temperature for 2 hours. After ethyl acetate was added, the reaction mixture was washed with saturated brine and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to give the title compound (14.0 mg).

Provenance & Evidence