Trifluoroacetic acid → HCID 57983534, compound

Participants

Reaction Steps

A solution of 1,1-dimethylethyl N-((7,8-dichloro-4-hydroxy-1,1-dimethyl-2-oxo-naphthalen-3-yl)carbonyl)glycinate (0.130 g, 0.314 mmol) in TFA (5.00 mL, 68.3 mmol) was stirred at 25° C. for 10 minutes. The resulting mixture was concentrated, azeotroped using DCM (2×100 mL), and dried in vacuo to give the title compound (0.0925 g). MS m/e=358 (M+H)+. Calculated for C15H13Cl2NO5 357.02.

Provenance & Evidence