Trifluoroacetic acid → HCID 57983451, compound

Participants

Reaction Steps

A solution of 1,1-dimethylethyl N-((6-chloro-1-(4-chlorophenyl)-4-hydroxy-1-methyl-2-oxo-naphthalen-3-yl)carbonyl)glycinate (0.675 g, 1.42 mmol) in TFA (10.0 mL, 127 mmol) was stirred at 25° C. for 10 minutes. The solution was concentrated, azeotroped in DCM (2×300 mL), and dried in a vacuum oven at 60° C. to give the title compound (0.580 g). MS m/e=420 (M+H)+. Calculated for C20H15Cl2NO5 419.03.

Provenance & Evidence