HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-(3,4-dichlorophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 3,4-Dichlorophenylacetic acid | HCID 79874 | — |
| Product | Methyl 2-(3,4-dichlorophenyl)acetate | HCID 1268257 | — |
Reaction Steps
2-(3,4-Dichlorophenyl)acetic acid (25.0 g, 122 mmol) was dissolved in MeOH (122 mL) at ambient temperature. Sulfuryl dichloride (8.89 mL, 122 mmol) was then added, and the mixture was stirred for 2 hours. The reaction mixture was concentrated in vacuo to give the title compound as a light yellow oil which was used without further purification. MS (m/z)=219 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928139B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-fed48536345c4a879e5cec7ca5124267 |
| Source note | uspto-grants-2011_04 |