Trifluoroacetic acid → HCID 57983491, compound

Participants

Reaction Steps

A solution of 1,1-dimethylethyl N-((8-chloro-4-hydroxy-1,1-dimethyl-2-oxo-naphthalen-3-yl)carbonyl)glycinate (0.162 g, 0.427 mmol) in TFA (5.00 mL, 67.3 mmol) was stirred at 25° C. for 10 minutes. The solution was concentrated, azeotroped using DCM (2×100 mL), and dried in vacuo to give the title compound (0.138 g). MS m/e=324 (M+H)+. Calculated for C15H14ClNO5 323.06.

Provenance & Evidence