Trifluoroacetic acid → HCID 57983452, compound

Participants

Reaction Steps

A solution of 1,1-dimethylethyl N-((6N-((7-chloro-8-fluoro-4-hydroxy-1,1-dimethyl-2-oxo-naphthalen-3-yl)carbonyl)glycinate (0.148 g, 0.372 mmol) in TFA (5.00 mL, 64.9 mmol) was stirred at 25° C. for 15 minutes. The solution was concentrated, azeotroped using DCM (2×100 mL), and dried in vacuo to give the title compound (0.128 g). MS m/e=342.4 (M+H)+. Calculated for C15H13ClFNO5 341.05.

Provenance & Evidence