HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 57900090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 57900484 | HCID 57900484 | — |
| Reactant | HCID 58265765 | HCID 58265765 | — |
| Product | HCID 57900090 | HCID 57900090 | — |
Reaction Steps
Following the procedure from Example 235, 8-bromo-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide was reacted with 3-chloro-4-hydrazinyl-N,N-dimethylbenzamide in acetic acid to give 342 as a colorless solid after purification by flash column chromatography (50-100% ethyl acetate in hexanes). MS: (ESI+) 531.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928248B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-4ffee14d231d4883aea627daf2efea8e |
| Source note | uspto-grants-2011_04 |