HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12066767, compound → HCID 86638523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12066767 | HCID 12066767 | — |
| Reactant | 2,5-Dimethoxy-3,4,6-trimethylphenol | HCID 19009254 | — |
| Product | HCID 86638523 | HCID 86638523 | — |
Reaction Steps
The process was carried out as described in point 5.4 above, using 0.812 g (4.362 mmol) of 2,5-dinitrofluorobenzene and 0.856 g (4.362 mmol) of 2,5-dimethoxy-3,4,6-trimethylphenol. The title product was obtained in the form of a yellow solid (1.412 g, 89%) after column chromatography using, as eluent, a 75:25 mixture of light mineral spirit (60-80° C.):diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932050B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-2a8fd293e62442659039dc1229325993 |
| Source note | uspto-grants-2011_04 |