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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2079448Generated: October 31, 2026

HCID 12066767, compound → HCID 86638523, compound

https://huagongshe.com/reaction/2079448

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12066767HCID 12066767—
Reactant2,5-Dimethoxy-3,4,6-trimethylphenolHCID 19009254—
ProductHCID 86638523HCID 86638523—

Reaction Steps

The process was carried out as described in point 5.4 above, using 0.812 g (4.362 mmol) of 2,5-dinitrofluorobenzene and 0.856 g (4.362 mmol) of 2,5-dimethoxy-3,4,6-trimethylphenol. The title product was obtained in the form of a yellow solid (1.412 g, 89%) after column chromatography using, as eluent, a 75:25 mixture of light mineral spirit (60-80° C.):diethyl ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07932050B2
Source datasetuspto-grants-2011_04
ORD IDord-2a8fd293e62442659039dc1229325993
Source noteuspto-grants-2011_04