2-Decalone → 1,3-Dimethyl-5-methylenecyclohexane

HRID 2079469Notes

Reaction equation

[CH3:1][CH:2]1[CH2:7][CH:6]([CH3:8])[CH2:5][C:4](=O)[CH2:3]1.[CH2:10]1CC2C(CC(CC2)=O)CC1>>[CH3:1][CH:2]1[CH2:7][C:6](=[CH2:8])[CH2:5][CH:4]([CH3:10])[CH2:3]1

Participants

Reactant 2

HCID 1003282-Decalone

HCID 1375443,5-Dimethylcyclohexanone

Product 1

HCID 155775961,3-Dimethyl-5-methylenecyclohexane

Procedure

The title compound was prepared as described in Example 45A substituting 3,5-dimethylcyclohexanone, commercially available from Aldrich, for 2-decalone.

Sources & evidence

ORD record: ord-afd4fa68bf214439bae2663be6465523
Source dataset: uspto-grants-2011_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07932245B2

Reaction notes

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