Ethyl Spiro[2.5]octane-1-carboxylate → 5,7-dimethylspiro[2.5]octane-1-carboxylic Acid

HRID 2079470Notes

Reaction equation

HRID 2079470 reaction equation
[CH3:1][CH:2]1[CH2:14][CH:13]([CH3:15])[CH2:12][C:4]2([CH:6]([C:7]([O:9]CC)=[O:8])[CH2:5]2)[CH2:3]1.C1(C(OCC)=O)C2(CCCCC2)C1>>[CH3:1][CH:2]1[CH2:14][CH:13]([CH3:15])[CH2:12][C:4]2([CH:6]([C:7]([OH:9])=[O:8])[CH2:5]2)[CH2:3]1

Participants

3

Reactant 2

HCID 11206164Ethyl Spiro[2.5]octane-1-carboxylateHCID 67102969Ethyl 5,7-dimethylspiro[2.5]octane-1-carboxylate

Product 1

HCID 100581675,7-dimethylspiro[2.5]octane-1-carboxylic Acid

Procedure

The title compound was prepared as described in Example 1B substituting the product from Example 21B for the product from Example 1A. MS m/z 182 (M+NH4)+.

Sources & evidence

ORD record
ord-ff88ab0a493141f696e5e637f76ca944
Source dataset
uspto-grants-2011_04
Patent number
US07932245B2

Reaction notes

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