Ethyl Spiro[2.5]octane-1-carboxylate → 2-Methylspiro[2.4]heptane-1-carboxylic acid

HRID 2079473Notes

Reaction equation

HRID 2079473 reaction equation
[CH3:1][CH:2]1[C:4]2([CH2:8][CH2:7][CH2:6][CH2:5]2)[CH:3]1[C:9]([O:11]CC)=[O:10].C1(C(OCC)=O)C2(CCCCC2)C1>>[CH3:1][CH:2]1[C:4]2([CH2:8][CH2:7][CH2:6][CH2:5]2)[CH:3]1[C:9]([OH:11])=[O:10]

Participants

3

Reactant 2

HCID 11206164Ethyl Spiro[2.5]octane-1-carboxylateHCID 67102630Ethyl 2-methylspiro[2.4]heptane-1-carboxylate

Product 1

HCID 104418982-Methylspiro[2.4]heptane-1-carboxylic acid

Procedure

The title compound was prepared as described in Example 1B substituting the product from Example 27A for the product from Example 1A. MS m/z 154 (M)+.

Sources & evidence

ORD record
ord-d58119cbc5f4469ea99bab3e08e62006
Source dataset
uspto-grants-2011_04
Patent number
US07932245B2

Reaction notes

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