Ethyl Spiro[2.5]octane-1-carboxylate → 680619-21-0

HRID 2079477Notes

Reaction equation

HRID 2079477 reaction equation
[CH:1]1([C:10]([O:12]CC)=[O:11])[C:3]2([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]2)[CH2:2]1.C1(C(OCC)=O)C2(CCCCC2)C1>>[CH:1]1([C:10]([OH:12])=[O:11])[C:3]2([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]2)[CH2:2]1

Participants

3

Reactant 2

HCID 11206164Ethyl Spiro[2.5]octane-1-carboxylateHCID 67103099HCID 67103099, compound

Product 1

HCID 10241191680619-21-0

Procedure

The title compound was prepared as described in Example 1B substituting the product from Example 39B for the product from Example 1A. 13C NMR (CDCl3, 100 MHz) δ 23.7, 26.2, 26.4, 27.2, 27.9, 28.0, 28.4, 31.2, 33.4, 33.5, 40.1, 179.3; MS m/z 168 (M)+.

Sources & evidence

ORD record
ord-175cbcaaa1094fcb829e797b12168998
Source dataset
uspto-grants-2011_04
Patent number
US07932245B2

Reaction notes

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