HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57657554, compound → Methyl 3-(4-chloro-2-(trifluoromethyl)phenyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57657554 | HCID 57657554 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 3-(4-chloro-2-(trifluoromethyl)phenyl)propanoate | HCID 53419598 | 99.2% |
Reaction Steps
A mixture of (E)-methyl 3-(4-chloro-2-(trifluoromethyl)phenyl)acrylate (5 g) and palladium on charcoal (10%, dry, 2 g) in ethyl acetate (50 ml) was stirred under balloon hydrogen pressure for 3 hours. After filtration, filtrate was concentrated to give methyl 3-(4-chloro-2-(trifluoromethyl)-phenyl)propanoate (5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932251B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-04587aef65dd4cf997fc751605d5d97a |
| Source note | uspto-grants-2011_04 |