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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2080055Generated: November 1, 2026

HCID 22118244, compound → HCID 23130679, compound

https://huagongshe.com/reaction/2080055

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22118244HCID 22118244—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 23130679HCID 2313067964%

Reaction Steps

10% Palladium-carbon (50 mg) was added to a solution of the resulting 6-phenoxy-pyridine-2-carbonitrile (100 mg, 0.51 mmol) in methanol (5.0 mL), the mixture was stirred at room temperature for 24 hours under hydrogen atmosphere (1 atm). The catalyst was removed by filtration, and the filtrate was concentrated to obtain the title compound (65 mg, 64%) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07932272B2
Source datasetuspto-grants-2011_04
ORD IDord-6cf3f745fbea453dacd81900205c47de
Source noteuspto-grants-2011_04