Sodium Azide → HCID 57433663, compound

Participants

Reaction Conditions

Reaction Steps

1.91 g of sodium azide was added to a dimethylformamide (10 ml) solution of 2.54 g of methyl 2-(acetyloxy)-4-[(methylsulfonyl)oxy]butanoate, and stirred under heat at 70° C. for 8 hours. The reaction liquid was restored to room temperature and extracted with ethyl acetate. The organic layer was washed with saturated saline water and dried, and the solvent was evaporated away under reduced pressure to obtain 2.70 g of methyl 2-(acetyloxy)-4-azidobutanoate as a brown oil.

Provenance & Evidence