Ethanol → HCID 67103750, compound

Participants

Reaction Conditions

Reaction Steps

Potassium ferricyanide (5.78 g) was dissolved in distilled water (40 ml) and the whole was heated to 90° C. A suspension containing the compound (1.09 g) obtained in Example 43-2, ethanol (1.0 ml), and a 30% sodium hydroxide aqueous solution (3.2 ml) was dropped to the reaction solution for 5 minutes. The whole was stirred at 90° C. for 3 hours and then cooled to room temperature. The precipitated solid was filtrated out and purified by recrystallization (methanol), thereby obtaining the subject compound (0.53 g) as a white solid.

Provenance & Evidence