HuagongsheHuagongshe Chemistry Print Report · For research reference only
77855-81-3 → HCID 101591932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 77855-81-3 | HCID 6440579 | — |
| Reactant | (6R,25R)-5-O-Demethyl-28-deoxy-6,28-epoxy-25-methylmilbemycin B | HCID 9828343 | — |
| Reactant | HCID 101591931 | HCID 101591931 | — |
| Product | HCID 101591932 | HCID 101591932 | 29% |
Reaction Steps
If milbemycin A3 or milbemycin D is reacted in an analogous manner, for example at a conversion rate of 10% a ratio of 40% 13β-hydroxymilbemycin A3 and 60% 14,15-epoxymilbemycin A3 is obtained or, at a conversion rate of 13%, a ratio of 29% 13β-hydroxymilbemycin D to 71% 14,15-epoxymilbemycin D is obtained (HPLC analysis).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183749 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-489d187bbc95423ba9b500c2908563fb |
| Source note | uspto-grants-1993_02 |