HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Dimethyldiphenylmethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,2-Bis-(4-methylsulphonyloxy-phenyl)-propane | HCID 14832825 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Dimethyldiphenylmethane | HCID 13065 | 84% |
Reaction Steps
0.5 mol of Compound A were stirred at 40° C. and under 20 bar of H2 in 3,000 ml of ethyl acetate with the addition of 27 g of palladium/carbon (5% Pd) and 1 mol of triethylamine; during the course of the reaction a further 15 g of Pd/C were added in total. After distillation, 84% of Compound B was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183926 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-c7d3291c9bc2418294004ed97bea36fc |
| Source note | uspto-grants-1993_02 |