HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 15070141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 15070125 | HCID 15070125 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15070141 | HCID 15070141 | 98.5% |
Reaction Steps
Under the conditions of example 9, a solution of 60 mg of 4-[2-[(1Z,3E)-(5RS)-5-hydroxy-1,3-tridecadienyl]-phenoxy]-butyric acid ethyl ester in 5 ml of methanol and 2 ml of 0.5 n sodium hydroxide solution is saponified, worked up and chromatographed on silica gel with n-hexane/ethyl acetate=98/2. 55 mg of the title compound is obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183925 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-99fe7c29ba8a4a639191d03e076b5b31 |
| Source note | uspto-grants-1993_02 |