HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → 1,1-Dimethyl-3-hydroxymethyl-1,2,5,6-tetrahydropyridinium p-toluenesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | 1-Methyl-1,2,5,6-tetrahydropyridine-3-methanol | HCID 424700 | — |
| Product | 1,1-Dimethyl-3-hydroxymethyl-1,2,5,6-tetrahydropyridinium p-toluenesulfonate | HCID 15052253 | 179.4% |
Reaction Steps
The procedures of Reference Example 10 were repeated using 2.8 g of 1-methyl-1,2,5,6-tetrahydro-3-pyridinemethanol and 4.1 g of methyl p-toluenesulfonate to give 6.19 g of the desired compound as a white crystalline product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183811 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-70cff4d2584345faa9ad73ddf7bacb69 |
| Source note | uspto-grants-1993_02 |