HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 2-Acetyloxy-1-benzyloxy-3-hexadecyloxybutane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Benzyloxy-3-hexadecyloxy-2-butanol | HCID 15052293 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Acetyloxy-1-benzyloxy-3-hexadecyloxybutane | HCID 15052294 | 95.7% |
Reaction Steps
In chloroform, 4.33 g of 1-benzyloxy-3-hexadecyloxy-2-butanol, 26.34 g of acetic anhydride and 10.42 g of triethylamine were heated under reflux for 17 hours. The reaction mixture was treated in a conventional manner and purified by silica gel column chromatography to give 4.56 g of 2-acetyloxy-1-benzyloxy-3-hexadecyloxybutane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183811 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-328f688d293640b4b7cd121287ffca28 |
| Source note | uspto-grants-1993_02 |