HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → [(4,7-Dimethylbenzoxazol-2-yl)methyl]-triphenylphosphonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 2-Chloromethyl-4,7-dimethylbenzoxazole | HCID 10035562 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | [(4,7-Dimethylbenzoxazol-2-yl)methyl]-triphenylphosphonium chloride | HCID 10027143 | — |
Reaction Steps
The product of Step A above was heated with an equimolar amount of triphenylphosphine in refluxing toluene for 15-25 hours to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185251 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-0ee0e72b845e4494964fb9b0fcce5b53 |
| Source note | uspto-grants-1993_02 |