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HRID2081548

反应详情

EQUATION

反应方程式

HRID 2081548 的结构方程式

REACTANTS

反应物

2
结构：CCOC=C(C(C)=O)C(C)=O
HCID240418

3-(ethoxymethylene)pentane-2,4-dione

C8H12O3

结构：Nc1ccc(C2=NNC(=O)CC2)cc1
HCID676750

6-(4-Aminophenyl)-4,5-dihydropyridazin-3(2H)-one

C10H11N3O

PRODUCTS

生成物

1
结构：CC(=O)C(=CNc1ccc(C2=NNC(=O)CC2)cc1)C(C)=O
HCID178467922

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A solution containing 0.38 g of 6-(4-aminophenyl)-4,5-dihydropyridazin-3(2H)one and 0.4 g of 3-ethoxymethylene-2,4-pentanedione in 5 ml of ethanol was refluxed for 1 h. Yield 0.3 g, mp 218°-222° C.

WORKUP

后处理

  1. temperaturewas refluxed for 1 h