HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → Tetradecanehydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Methyl Myristate | HCID 31284 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Tetradecanehydrazide | HCID 2748033 | 43.9% |
Reaction Steps
Hydrazine (1.9 mL, 0.058 mol) was added to a solution of methyl tetradecanoate (13.96 g, 0.058 mol) in methanol (300 mL) and the solution refluxed for 3 days. The mixture was allowed to cool and filtered to yield 6.17 g of a crystalline solid, m.p. 107°-111° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185358 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-afcf65b2ba08436fa2698374f5ed43d2 |
| Source note | uspto-grants-1993_02 |