HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 14749935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | HCID 14749912 | HCID 14749912 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14749935 | HCID 14749935 | — |
Reaction Steps
A mixture of 20.0 g (51 mMole) 2-hydroxymethyl-5-octadecyloxy-4-pyranone and 30 mL of a 40% solution of propylamine in ethanol is heated in an autoclave at 100°-110° C. for 5 hours. After cooling, the crystallizate formed is taken up in water, stirred, filtered off, dried and recrystallized from ethyl acetate, colorless crystals thereby being obtained; m.p. 120°-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185352 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-d955f5454bec433d8653aa15069efe7e |
| Source note | uspto-grants-1993_02 |