Acetylacetone → HCID 19780557, compound

HRID 2081715Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([N+:12]([O-:14])=[O:13])[CH:11]=1)[CH:7]=O)([O-:3])=[O:2].[CH3:15][C:16](=[O:21])[CH2:17][C:18](=[O:20])[CH3:19]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:7]=[C:17]([C:16](=[O:21])[CH3:15])[C:18](=[O:20])[CH3:19])[CH:9]=[C:10]([N+:12]([O-:14])=[O:13])[CH:11]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 31261Acetylacetone

HCID 17123033,5-dinitrobenzaldehyde

Product 1

HCID 19780557HCID 19780557, compound

Procedure

The procedure described in Example 1 was repeated by using 2.53 g 3,5-dinitrobenzaldehyde and 2.43 g of 2,4-pentanedione. Yield 0.8 g, mp 101°-105° C.

Sources & evidence

ORD record: ord-b803fbc50ee848d49a98c8a57c75d2d8
Source dataset: uspto-grants-1993_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05185370

Reaction notes

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