3,5-Heptanedione → HCID 19096383, compound

HRID 2081722Notes

Reaction equation

[C:1]([C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH:6]=O)#[N:2].[CH3:11][CH2:12][C:13](=[O:19])[CH2:14][C:15](=[O:18])[CH2:16][CH3:17]>>[C:1]([C:3]1[CH:4]=[C:5]([CH:6]=[C:14]([C:13](=[O:19])[CH2:12][CH3:11])[C:15](=[O:18])[CH2:16][CH3:17])[CH:8]=[CH:9][CH:10]=1)#[N:2]

Participants

Reactant 2

HCID 819233,5-Heptanedione

HCID 90670m-Formylbenzonitrile

Product 1

HCID 19096383HCID 19096383, compound

Procedure

The procedure described in Example 19 was repeated by using 1.82 g 3-cyanobenzaldehyde and 3.5 g 3,5-heptanedione. Yield 0.4 g, mp 51°-52° C.

Sources & evidence

ORD record: ord-301f64e037bc477793017a52879be181
Source dataset: uspto-grants-1993_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05185370

Reaction notes

Loading…