HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4-Chloro-1-nitro-2-phenoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2,4-Dichloronitrobenzene | HCID 11899 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | 4-Chloro-1-nitro-2-phenoxybenzene | HCID 12290044 | — |
Reaction Steps
Aryl ethers have been formed by reacting aryl halides with phenols under various conditions. Roberts and Turner disclose (J. Chem. Soc., 1925, 127, p. 2004) that 2,4-dichloronitrobenzene reacts with phenol in aqueous KOH, at 100° C., to give a quantitative yield of 4-chloro-2-phenoxynitrobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185471 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-e3603f098c944935bd32cbf607d2af6f |
| Source note | uspto-grants-1993_02 |