HCID 5095316, compound → HCID 19779074, compound

HRID 2081937Notes

Reaction equation

HRID 2081937 reaction equation
[CH2:1]([S:13]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[N+:22]([O-])=O)(=[O:15])=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].NC1C=CC=CC=1C(OCCCCCCCCCCCC)=O>>[CH2:1]([S:13]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[NH2:22])(=[O:15])=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 5095316HCID 5095316, compoundHCID 19779079HCID 19779079, compound

Product 1

HCID 19779074HCID 19779074, compoundYield 93.6%

Procedure

50.9 g of light yellow oily 2-dodecylsulfonylaniline was prepared from 59.4 g of the foregoing 2-dodecylsulfonylnitrobenzene in the same manner as dodecyl o-aminobenzoate in Synthesis Example 2. Yield 93.5%.

Sources & evidence

ORD record
ord-54ddb4dc8c0e43ad82f156684e06cf06
Source dataset
uspto-grants-1993_02
Patent number
US05187055

Reaction notes

Loading…