HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86438, compound → HCID 54473635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86438 | HCID 86438 | — |
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54473635 | HCID 54473635 | 59% |
Reaction Steps
16.6 g (41 mmol) of Lawesson's reagent were added to 10.2 g (33 mmol) of 2-[2-methylphenoxymethyl]-phenylglyoxylic acid methyl ester O-methyloxime in 50 ml of xylene. Refluxing was carried out for 24 hours and the solvent was removed under reduced pressure. Chromatography over silica gel using ethyl acetate/hexane gave 6.3 g (59%) of the compound as a black oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187170 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-ba51251bb5e7401d9daea8494be72922 |
| Source note | uspto-grants-1993_02 |