Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-tert-Butylbenzylamine | HCID 2735655 | — |
| Reactant | Ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide | HCID 54498586 | — |
| Product | Tebufenpyrad | HCID 86354 | — |
Reaction Steps
A mixture of ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide and 4-tert-butylbenzylamine is heated to 200° C. for four hours with continuous stirring. Thereafter the reaction mixture is cooled to room temperature and the reaction mixture purified by silica gel chromatography to obtain the desired product 115°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05187184 |
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| Source dataset | uspto-grants-1993_02 |
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| ORD ID | ord-644c9dc91c47401fa1b452f761d7dbde |
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| Source note | uspto-grants-1993_02 |
|---|
