HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 178441897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | HCID 10068546 | HCID 10068546 | — |
| Product | HCID 178441897 | HCID 178441897 | 40% |
Reaction Steps
Reaction of 2-butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-5,6-dimethyl-3H-imidazo[1,2-b][1,2,4]triazole (from Step B) with trimethyltin azide according to the procedure of Example 1, Step G, furnished a 40% yield of the title compound as a light tan solid, mp 138°-141° C.; homogeneous by TLC in 90:10:0.1 CH2Cl2 -MeOH-AcOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187179 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-fae8b21089d34ebd93027a134319f3c3 |
| Source note | uspto-grants-1993_02 |