HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-D-Trp(CH2CO2Et)-OBzl → Boc-D-Trp(CH2CO2Et)-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-D-Trp(CH2CO2Et)-OBzl | HCID 131717763 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Boc-D-Trp(CH2CO2Et)-OH | HCID 131717764 | 91% |
Reaction Steps
To a solution of Boc-D-Trp(CH2CO2Et)-OBzl (4.14 g) in ethanol (60 ml) was added 5% palladium on carbon (0.7 g) and the mixture was hydrogenated for one and half an hour under atmospheric pressure. Filtration of the catalyst and concentration of the filtrate under vacuum gave Boc-D-Trp(CH2CO2Et)-OH as an amorphous solid (3.06 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187156 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-fd6a5b44456442b6b07a2549bc29ec31 |
| Source note | uspto-grants-1993_02 |