HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 73345468, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 131717781 | HCID 131717781 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 73345468 | HCID 73345468 | — |
Reaction Steps
A solution of Z-Gly-Thr-D-Trp(CHO)-Phe-NMeBzl (560 mg) in a mixed solvent of ethanol (30 ml) and acetic acid (10 ml) was hydrogenated over 10% palladium on carbon (350 mg) under atmospheric pressure for two hours. After filtration of the catalyst and evaporation, the residue was dissolved in water (50 ml) and lyophilized to give H-Gly-Thr-D-Trp(CHO)-Phe-NMeBzl.AcOH (230 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187156 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-40abb0c8633141c1b1e624ee9b56cfd4 |
| Source note | uspto-grants-1993_02 |