HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethynylcyclohexane → 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethynylcyclohexane | HCID 70263 | — |
| Reactant | 2-Iodoadenosine | HCID 169662 | — |
| Reactant | (Prop-2-yn-1-yl)cyclopentane | HCID 521007 | — |
| Product | 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine | HCID 132348 | 70.3% |
Reaction Steps
The procedure of Example 1 was repeated except that 1.56 g (3.98 mmol) of 2-iodoadenosine was used as the starting compound and that the cyclohexylacetylene was replaced by 3-cyclopentylpropyne, whereby 1.05 g (2.8 mmol) of crystalline 2-(3-cyclopentyl-1-propynyl)adenosine was obtained (yield: 70.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189027 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-c4dab15d462d4976a7538035653ba803 |
| Source note | uspto-grants-1993_02 |