Fumaric Acid → HCID 19761235, compound

HRID 2082348Notes

Reaction equation

HRID 2082348 reaction equation
[C:1]1([CH2:9][N:10]2[CH2:15][CH2:14][CH:13]([N:16]([CH3:24])[C:17](=[O:23])[O:18][CH2:19][CH:20]([CH3:22])[CH3:21])[CH2:12][CH2:11]2)[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH:2]=1.[C:25]([OH:32])(=[O:31])/[CH:26]=[CH:27]/[C:28]([OH:30])=[O:29]>C(O)C>[C:25]([OH:32])(=[O:31])/[CH:26]=[CH:27]/[C:28]([OH:30])=[O:29].[C:1]1([CH2:9][N:10]2[CH2:11][CH2:12][CH:13]([N:16]([CH3:24])[C:17](=[O:23])[O:18][CH2:19][CH:20]([CH3:22])[CH3:21])[CH2:14][CH2:15]2)[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH:2]=1

Participants

4

Reactant 2

HCID 444972Fumaric AcidHCID 19761236HCID 19761236, compound

Product 1

HCID 19761235HCID 19761235, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The isobutyl N-[1-(benzocyclobuten-1-ylmethyl)-piperid-4-yl]-N-methylcarbamate so obtained is then converted into a salt with an appropriate amount of fumaric acid in ethanol.

Sources & evidence

ORD record
ord-f1ade4a4c67e4cffacad0a92ea273a4c
Source dataset
uspto-grants-1993_02
Patent number
US05189045

Reaction notes

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