2-Methoxyethyl chloroformate → HCID 19761241, compound

HRID 2082350Notes

Reaction equation

HRID 2082350 reaction equation
[CH2:1]([N:8]1[CH2:13][CH2:12][CH:11]([N:14]([CH3:22])[C:15](=[O:21])[O:16][CH2:17][CH2:18][O:19][CH3:20])[CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:23]C(O[CH2:27][CH2:28]OC)=O>>[ClH:23].[C:2]1([CH2:1][N:8]2[CH2:9][CH2:10][CH:11]([N:14]([CH3:22])[C:15](=[O:21])[O:16][CH2:17][CH2:18][O:19][CH3:20])[CH2:12][CH2:13]2)[C:7]2[CH:6]=[CH:5][CH:4]=[CH:3][C:28]=2[CH:27]=1

Participants

3

Reactant 2

HCID 694002-Methoxyethyl chloroformateHCID 19761196HCID 19761196, compound

Product 1

HCID 19761241HCID 19761241, compound

Procedure

This compound was prepared in accordance with the process described in Example 11 (Stages B and C) but using 2-methoxyethyl N-(1-benzylpiperid-4-yl)-N-methylcarbamate in Stage B. The latter is obtained in accordance with the process described in Stage B of Example 1 using methoxyethyl chloroformate instead of propionyl chloride.

Workup

  1. customThis compound was prepared in accordance with the process
  2. customThe latter is obtained in accordance with the process

Sources & evidence

ORD record
ord-26239d14fc3a48dcbdcdfacf5eeefdf3
Source dataset
uspto-grants-1993_02
Patent number
US05189045

Reaction notes

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